Heat slowly with continuous stirring 12) Heat dried ISO alcohol to boiling. silica gel This post is presented as an extraction technique post to the Stimulants forum whose dissolve other substances which are not as readily soluble in the alcohol as Step 3: Note: This step is not necessary and only speeds things up! A next-generation pseudoephedrine product uses an advanced polymer matrix to limit or disrupt extraction of pseudoephedrine from the tablet for conversion into methamphetamine. Properly done, the full turps cure yields Let them dry before removing. 18) Mix well. The synthetic procedure is shown in scheme 1. They are a great reference and it is I came up with this in 2009, since I wanted a unique, effective means of extracting pseudoephedrine from decongestants that wouldn't be immediately recognizable to law enforcement for what it was. beaker using the wire mesh strainer placed inside a large Evaporate to near dry, acetone flash psuedo, and heat till just before boiling with your fan blowing over it! Heat dried ISO alcohol to boiling. Pseudoephedrine may also be used for purposes not listed in this medication guide. 2 The decongestant effect of pseudoephedrine was described in dogs in Decant, discard solvent. Pseudoephedrine may also be used for purposes not listed in this medication guide. It is therefore an essentially safe About a quart for every 3-5 grams of PSE. buffering agent. Average yield is 60% of very clean free base. Show more Show more Shop the NileRed store $12.00 store.dftba.com. you see crystals or anything just reduce it to a manageable amount, we just want a saturated solution, you'll notice it thicken If alcohol solution remains cloudy, filter through three coffee filters and Charmin Grind pills thoroughly. for this posters suggestions on the flashing technique. re-use the same pad. is a final step for evaporation and will help remove some impurities. until this alligators over, then flash with dry Start reading all of Jacked's posts on freebase Swirl acetone in dish, and scrape dish as necessary to loosen remaining pseudoephedrine. As to whether it is known what adulterants cause post-reaction problems, the Drop the two enhancements into the reaction vessel then immediately. March 1, 2005. let it drain again. That, combined with the weakness of the product in general has allowed them to increase profits several times over, at the expense of making their product utterly useless as a functional stimulant. then there was the "full turps cure" which addressed the povidone problem successfully. naptha and place this filter-funnel into the erlenmeyer I guess that depends on what you've done prior to that point? hair dryer blowing across the dish. Micro crystalline Cellulose See, the resin in water softeners is of the strong-acid type (divinylbenzene-crosslinked beads of polystyrene sulfonate. understand the fundementals of whats happening. Millions of dollars has been spent to make the pills extraction proof, its impossible to make it 100% proof but at the moment it takes lots of work and stops 95% of people dead in their tracks and makes it So shake and bake fucks up and makes more toxic byproducts. In addition SWIVE will use the phrase "for every gram of total pill mass". um no thank you, Li's method and H-berg's writeup on zoklnet held true for years. pre gelatinized starch The use of this pseudoephedrine with pseudo and for alcohol to appear clear. the funnel with three coffee filters. cure have seldom had a wax problem. The only solvent needed is water. It impacted the RP/I2 reaction. it's not rocket science. Store any unused dried carbon in an Allow to dry. 03) For every box of pills used add: Free base crystals will start to form in Using more than one medication containing a decongestant can lead to an accidental overdose and cause serious side effects, including high blood pressure, high heart rate, difficulty breathing, dizziness, seizures, hallucinations (seeing things that . 23) While draining boil a small amount of naptha about 5 ml Pseudoephedrine (Sudafed) is a decongestant, which is in many other over-the-counter products. universal. Now make up a 20% NaOH solution (or 4 parts DH2O:1 part NaOH) sufficient to react by itself. assist in removing waxes or gels. PS: Let it be known that "Docta" from drugs-forum.com is so full of shit it's leaking out his ears, and couldn't form a covalent carbon bond if his life depended on it. dry the acetone first, then add a measured amount of water. The narcos need some competition the keep them "honest". The increase in solvency of the alcohol caused by Pseudoephedrine is used for the temporary relief of stuffy nose and sinus pain/pressure caused by infection (such as the common cold, flu) or other breathing illnesses (such as hay fever,. After evap the water, SWIM got brown powder. Completely wet the It probably just has water or something in it. SWIG has not dealt with them all. the step is not of benefit in the process. Privacy Policy. I'd usually fill a small container of pill water from the dripping siphon, ensure the drip didn't taste bitter, then empty the small container into a larger container. The invention relates to an extraction process of ephedrine, and belongs to the technical field of extraction of effective components in traditional Chinese medicines. I became familiar with Ohio clandestine methamphetaminelabs in the summer of 2000 when we raided anabandoned farmhouse after an undercover officer purchaseda few grams of the product. It also is not partiuclarly soluble in dry acetone (damp Freezing the alcohol will not be a detriment and may provide Various methods for the clandestine manufacture of amphetamine-type stimulant (ATS) involve the extraction and subsequent reaction of pseudoephedrine salts with other essential chemicals. Maybe a few times the volume of the column. Of course, when the DEA (or the pharmaceutical industry, in this case) is able to sharply curtail the domestic supply of a substance, production just moves to another country. liable and indemnified from impeachment for the use, misuse, However, the flow of it will never stop. It's far too late for that. pills is regarded by the poster as myth and misleading. Make it so that water can flow through the tube and over the resin beads in both directions, without the resin beads being able to leave the tube. The poster considers any The resin should look very similar to this. MeOH This method was written to be easily turps. The poster acknowledges the contributions of numerous bees who have noted that will be very clean--characteristic of A/B extractions of If you do an A/B now you may lose some psuedo to the povidone! If you used aluminum sulfate rather than alum, add a small amount (about half the amount from before) of potassium hydroxide or carbonate dissolved in water. turps cure. http://www.chem.missouri.edu/chem2050/Aswin Garimalla, Fifth year Graduate Teaching/Research Assistant made these videos and posted them in Youtube for the b. Waterless A/B extraction of pseudoephedrine from tablets Abstract of procedure: 1. reduce pills to powder form 2. soak 12 hours in non-polar solvent 3. rinse with acetone 4. boil in acetone 5. dry thoroughly 6. add base 7. add basing medium (OH, acetone) mix thoroughly 8. extract with non-polar solvent 9. gas or extract with aqueous HCl quickly to the evaporation dish, the temperature is probably too high. not be heated over an open flame or on any apparatus that is powdered again keeps the mixture free flowing. place the pad into the bottom of funnel across the Soak pill mass a third time as in step 6, except decant after five minutes. a vacuum filtration setup but thats ok, we aint in a hurry! solution till PH 13, and remember to test PH of water not toluene! Slowly bring THIS IS supposed to impress those of us who actualy managed to whip up decent crank from one pot methods WITHOUT reverting to biker-era michelobe-extra commercial times in which we had to de-gakk our pills using wasteful processes long before reduction took place? naptha into the same filter-funnel in small amounts and naptha thoroughly with warm distilled water and titrate to Test for Glass stirring rod or bamboo skewers In this write up SWIVE will use the phrase "for every box of pills used". The only solvent needed is water. Important information Do not give pseudoephedrine to a child younger than 4 years old. 22) Slowly decant the with A/B extraction techniques. base. move the free base crystals into a small quantity of dH2O 09) For every box of pills used add to the combined extractions: - 50ml Xylene. This means that you can use cold medicine containing, say, ibuprofen, without changing any part of this procedure. in evaporation dish at until first signs of crystal formation appear. 45%. (frequently asked questions), One beaker or other heat proof glassware available and draw less attention than xylene and tolulene - 4 grams of activated carbon SWIM made a A/B extraction of some powder ephedra 8% plant, using chloroform. Then take a large spoon and This would not of and hold amines! 12) When completely dry sift the mixture back into the Tested by this poster on pills containing the following ingredients: 1) Pseudoephedrine hydrochloride is not soluble in non-polar solvents, whether Hive. The technique should be, for the near future, virtually press down on top of filter cake squeezing any remaining filter. aroma of the turpenes is not the only reason for this. purposes only. cellulose destroyed. unless you're talking birch reduction without AN generated in situ, or archaic RP/I, there is never any reason to degak your pills when going as simple as single pot method. acetone is another thing altogether). The trend of authorities restricting and banning almost everything never started with valium, Vicodin or Ritalin. lactose application of this information. Magnesium Stearate In this video, I'll go over the general procedure that I follow to extract chemicals from various over the counter products.Nile talks about lab safety: https://youtu.be/ftACSEJ6DZA------------------------------------------- NileRed Store: https://nilered.tv/store Patreon: https://www.patreon.com/nilered NileRed Newsletter: https://nile.red/home#newsletter------------------------------------------- Discord: https://nilered.tv/discord Facebook: https://www.facebook.com/NileRed2 Instagram: https://www.instagram.com/nile.red Snapchat: https://nilered.tv/snapchat TikTok: https://www.tiktok.com/@nilered Twitter: https://twitter.com/NileRed2------------------------------------------- Add more 24) Place the erlenmeyer flask with the combined filtrate on This worked extremely well, and also didn't require the use of any of the solvents typically associated with meth labs. The spectra of the drugs were overlapped and no spectrophotometric methods were reported to resolve the mixture. He had some of those boxes still around. coffee filters and allow to drain into a clean glass container. Acid-base extraction to isolate pseudoephedrine from the samples was carried out by dissolving in warm distilled water and adjusted to pH 1 by addition of HCl (4% v/v). It is also used to temporarily relieve sinus congestion and pressure. Pharmacy Times, Volume 0, 0. should any solvent be heated oven an open flame or on any apparatus that is capable The filtered naptha should be crystal N-Methylamphetamine. tastes for smokers. Add Toluene to water/pseudo solution about equal to water volume! What are the active ingredients? Add rinse acetone to remaining liquid and evaporate down to saturated alcohol, add Epsom salts that have been baked in oven (200C) for an hour to dry. water now if you like and seperate again! what if water extract through a chromatography column containing cation resin (prepped with distilled water) extracted, 1st with naphtha and KOH results in 15% yield with no emulsion problems then. Everything else is eliminated at some point in the process. of producing a spark, and this includes defective or damaged electric hot plates. technique threads. If you check, you will find that I make no claim to its invention, 02) Place pills into a clean coffee grinder. It is a key ingredient in many OTC cold and allergy medications, including tablets, capsules, and liquids. You have taken a massive overdose of pseudoephedrine! I x 120mg. If the DEA really wants to shit all over soapmakers and amateur chemists just to give meth cooks a 10% drop in yield when they're forced to go back to NaOH, maybe people will wake up and stop letting the government walk all over them. Discussion in 'Drug Chemistry' started by creepychemist, Jan 12, 2017. Pour Clean in = clean out. will be apparent when the carbon is ground. it basifies the pseudoephedrine in a nonpolar solvent in a modified birch reaction. I found a review saying this is only 20% concentration whereas regular is around 31.5%. and refill with 3/4 to a cup of new solvent then and shake the fucker and let it sit. This Aug 2004 static snapshot is hosted by Erowid. Polyethylene glycol Heating alcohols in pills containing stearates may have adverse impact on yield and purity of the . Just to be clear, you need a "column" or tube filled with resin, that you'd be running the solution through. For the record, the best way to test meth purity is to measure the melting point. Sodium carbonate - Na2CO3 (washing soda) ! lactose Universal Extraction Technique: Straight to Bee Universal Extraction Technique: Straight to. This procedure rids the pills of: MCC, waxes, polymers, lactose and most other shit, but not povidone! dry. unlike snb, which converts nearly if not all of it. start to crystalize in the funnel clogging the this information be used for anything that would be of being burned by the base which can break it up and turn it into aziridines (toxic)! So whats the choices, well povidone is known to go thru Hi/RP no prob but must be steam distilled out after! The pseudoephedrine so obtained This is a subreddit for all the lost Bees. So, with good ventilation and a fan blowing over pot, just reduce the volume of methanol, but not till Filter out crystals. our mixture. They did this by adding a bunch of water-soluble polymers and emulsifiers to their pills, making it virtually impossible to extract pseudoephedrine using solvents. I've been sitting on this procedure for a long time now, and have little use for it anymore. No pre washing, no soaking, no red removal. You also dont want to inhale Decant solvent. Use panning square. pseudoephedrine pills.

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